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Beilstein J. Org. Chem. 2017, 13, 543–551, doi:10.3762/bjoc.13.52
Graphical Abstract
Figure 1: Reaction scheme for the synthesis of eosin Y (2) and eosin B (4).
Figure 2: Reaction scheme for the synthesis of eosin-appended β-CDs, 2–β-CD and 4–β-CD (NMM: N-methylmorpholi...
Figure 3: TLC analysis of the composition of the crude coupling reaction mixtures.
Figure 4: 1H NMR spectrum of 2–β-CD with partial assignment (DMSO-d6, 600 MHz, 298 K).
Figure 5: Size distributions of 1 mM aqueous solutions of conjugates 4–β-CD (a) and 2–β-CD (b) at 25.0 °C (pH...
Figure 6: Normalized absorption spectra of aqueous solutions of (a) eosin Y (2) and (b) conjugate 2–β-CD and ...
Figure 7: Time-resolved fluorescence observed for aqueous solutions of (a) eosin Y (2) and (b) the 2–β-CD con...
Figure 8: 1O2 luminescence detected upon 528 nm light excitation of D2O solutions of (a) eosin Y (2) and (b) 2...
Beilstein J. Org. Chem. 2014, 10, 3152–3160, doi:10.3762/bjoc.10.332
Figure 1: Structure of RAMEA.
Figure 2: Structures of ALA, EPA and DHA.
Figure 3: Solubility of n−3 PUFAs and cholesterol in water solutions of 20% randomly methylated α-, β- and γ-...
Figure 4: The effect of n−3 PUFAs on the expression of CD1a cell surface protein in resting (red), LPS-activa...
Figure 5: Effect of n−3 PUFAs on the expression of the CD83 activation marker in resting (red), LPS-activated...
Figure 6: Effect of n−3 PUFAs on the expression of the pro-inflammatory cytokine IL-6 in moDC activated by LP...
Figure 7: The effect of n−3 PUFAs on the expression of GPR120 receptor in resting (red), LPS-activated (yello...
Beilstein J. Org. Chem. 2014, 10, 3007–3018, doi:10.3762/bjoc.10.319
Scheme 1: Schematic representation of the various synthetic routes for the introduction of an anchoring group...
Scheme 2: Synthetic strategy for the rhodaminylation of β-CD polymer.
Figure 1: TLC study of β-CD iodination showing the proceeding of 6-monoiodination with increasing reaction ti...
Figure 2: HSQC-DEPT spectrum of compound 1 with partial assignment.
Figure 3: IR spectra of compound 1 (black line) and compound 2 (red line) showing the disappearance of the az...
Scheme 3: Schematic representation for the coumarinylation of methylated β-CD-polymer, n, m, p and q mean the...
Figure 4: HSQC-DEPT spectra of compound 4 with partial assignment; in the upper part the full spectrum is sho...
Scheme 4: Schematic representation for the introduction of NBF in a cationic β-CD-polymer.
Scheme 5: Schematic representation for the introduction of fluorescein into a β-CD-polymer.